Chemical synthesis in reaction autoclave

Reaction Autoclave

The reaction autoclave with a thermostat Julabo is used for a wide range of chemical syntheses from hydrogenation, hydrothermal syntheses to reactions at low temperatures. It is used especially in the cases when high temperature and pressure is needed.

Acquired information
  • Carrying out of high-pressure and/or high temperature chemical synthesis
  • Synthesis under optional atmosphere
Sample types
  • Liquid or powder materials
  • Inorganic, organic or coordination compounds
Modes, conditions and precision
  • 3 reaction vessels can be used – stainless steel (50 mL) and two glass vessels (50 and 300 mL)
  • Temperature range 0–220°C, depending on the vessel used
  • The range of pressures from 1 up to 60 bars, depending on the vessel used
  • Stirrer rotation up to 3000 min–1
  • Inert (e.g. N2) or hydrogen atmosphere for hydrogenation reactions
  • Possibility of sampling during a reaction
  • Possibility of adding liquid or solid reactants during syntheses
  • Changing and programming the temperature gradients in a given range (suitable for e.g. controlled crystallization)

Any additional information on request: rcptm.services@upol.cz