Reaction Autoclave

The reaction autoclave with a thermostat Julabo is used for a wide range of chemical syntheses from hydrogenation, hydrothermal syntheses to reactions at low temperatures. It is used especially in the cases when high temperature and pressure is needed.
Acquired information
- Carrying out of high-pressure and/or high temperature chemical synthesis
- Synthesis under optional atmosphere
Sample types
- Liquid or powder materials
- Inorganic, organic or coordination compounds
Modes, conditions and precision
- 3 reaction vessels can be used – stainless steel (50 mL) and two glass vessels (50 and 300 mL)
- Temperature range 0–220°C, depending on the vessel used
- The range of pressures from 1 up to 60 bars, depending on the vessel used
- Stirrer rotation up to 3000 min–1
- Inert (e.g. N2) or hydrogen atmosphere for hydrogenation reactions
- Possibility of sampling during a reaction
- Possibility of adding liquid or solid reactants during syntheses
- Changing and programming the temperature gradients in a given range (suitable for e.g. controlled crystallization)
Any additional information on request:
rcptm.services@upol.cz