Chemical synthesis in reaction autoclave

Reaction Autoclave

The reaction autoclave with a thermostat Julabo is used for a wide range of chemical syntheses from hydrogenation, hydrothermal syntheses to reactions at low temperatures. It is used especially in the cases when high temperature and pressure is needed.

Acquired information

  • Carrying out of high-pressure and/or high temperature chemical synthesis
  • Synthesis under optional atmosphere

Sample types

  • Liquid or powder materials
  • Inorganic, organic or coordination compounds

Modes, conditions and precision

  • 3 reaction vessels can be used – stainless steel (50 mL) and two glass vessels (50 and 300 mL)
  • Temperature range 0–220°C, depending on the vessel used
  • The range of pressures from 1 up to 60 bars, depending on the vessel used
  • Stirrer rotation up to 3000 min–1
  • Inert (e.g. N2) or hydrogen atmosphere for hydrogenation reactions
  • Possibility of sampling during a reaction
  • Possibility of adding liquid or solid reactants during syntheses
  • Changing and programming the temperature gradients in a given range (suitable for e.g. controlled crystallization)

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